{"id":72682,"date":"2022-08-23T15:09:10","date_gmt":"2022-08-23T12:09:10","guid":{"rendered":"https:\/\/icia.ro\/?page_id=72682"},"modified":"2024-06-12T09:07:38","modified_gmt":"2024-06-12T06:07:38","slug":"multipass","status":"publish","type":"page","link":"https:\/\/icia.ro\/en\/multipass\/","title":{"rendered":"MULTIPASS"},"content":{"rendered":"<p><strong>Project title<\/strong>: Simultaneous elemental microanalytical method for environment and food control using passive sampling coupled with miniaturized instrumentation based on plasma microtorch optical emission spectrometry<\/p>\n<p><strong>Acronym<\/strong>: MULTIPASS<\/p>\n<p><strong>Contract no<\/strong>: 733PED \/ 27.06.2022<\/p>\n<p><strong>Contracting Authority:<\/strong> Executive Agency for Higher Education, Research, Development and Innovation Funding (UEFISCDI), P2 &#8211; Increasing the competitiveness of the Romanian economy through RDI<\/p>\n<h3>Abstract<\/h3>\n<p>The project aims to develop and validate new highly-sensitive microanalytical methods without matrix effects to determine Hg, Pb, Cd, As, Sb, Cu and Zn of interest for environmental and food quality control using passive preconcentration by gradient diffusion in thin layer (DGT) and detection by optical emission spectrometry in capacitively coupled plasma microtorch (DGT-SSETV-\u03bcCCP-OES). The starting level of the project is TRL3 through the existence of the miniaturized spectrometric experimental model and the TRL4 level is reached by validation of the methods applied to environmental and food samples. The duration of the project is 24 months, in two stages, and is carried out in partnership by Research Institute for Analytical Instrumentation Cluj-Napoca (CO-ICIA), Babes-Bolyai University Cluj-Napoca (P1-UBB) and Technical University Cluj-Napoca (P2-UTCN). The first stage is intended to increase the technological maturity of the SSETV-\u03bcCCP-OES system at TRL4 by in-situ and ex-situ DGT preconcentration. The preconcentration and spectral detection will be optimized in such a way as to develop simultaneous multielemental methods. Analytical performances will be compared with traditional methods based on inductively coupled plasma optical emission spectrometry, graphite furnace atomic absorption and thermal desorption atomic absorption spectrometry. The second stage is dedicated to the development and validation of DGT-SSETV-\u03bcCCP-OES microanalytical methods compared to traditional methods and European Commission requirements for official control laboratories. The analytical capability will be presented to potential users through a practical demonstration. The standard operating procedures will be implemented in the CO-ICIA and P1-UBB laboratories. The results will be disseminated through 4 articles in WoS journals and participation in conferences (4 national and 6 international). An application for a national patent will be considered.<\/p>\n<h3>Project objective<\/h3>\n<p>The main objective of the MULTIPASS project is to develop new microanalytical methods as TRL4 for the simultaneous determination of priority hazardous elements (Pb, Cd, Hg) and other elements (As, Sb, Se, Cu, Zn) in environment and food microsamples using a fully miniaturized laboratory experimental model based on direct liquid microsampling SSETV-\u03bcCCP-OES in tandem with DGT device for in-situ and ex-situ preconcentration and analyte separation.<\/p>\n<h3>Estimated results<\/h3>\n<ul>\n<li>Testing and optimization report on the working conditions for in-situ and ex-situ preconcentration of Hg, Pb, Cd, As, Sb, Se, Cu and Zn using the DGT devices;<\/li>\n<li>Optimization report on the working conditions for SSETV as device for direct liquid microsampling after DGT preconcentration;<\/li>\n<li>Software to control the thermal program of the Rh filament;<\/li>\n<li>Optimization report on the working conditions for plasma microtorch interfaced with a low resolution microspectrometer for simultaneous multielemental determination by DGT-SSETV-\u03bcCCP-OES;<\/li>\n<li>Report on improved analytical performance (limit of detection, quantification, and compensation of non-spectral effects) for DGT-SSETV-\u03bcCCP-OES methods in low power plasma microtorch after DGT analytes preconcentration\/separation compared to direct liquid microsampling without DGT;<\/li>\n<li>Comparative study of analytical performance of DGT-SSETV-\u03bcCCP-OES with traditional methods, GFAAS, TDAAS, ICP-OES and European Legislations demands for official laboratory control;<\/li>\n<li>Validation report for microanalytical methods based on DGT-SSETV-\u03bcCCP-OES for simultaneous multielemental determination in environmental samples;<\/li>\n<li>Validation report for microanalytical methods based on DGT-SSETV-\u03bcCCP-OES for simultaneous multielemental determination in food samples;<\/li>\n<li>Microanalytical methods for environmental samples using DGT preconcentration and multielemental determination by implementation of DGT-SSETV-\u03bcCCP-OES as TRL4 on real samples;<\/li>\n<li>Microanalytical methods for food samples using DGT preconcentration and multielemental determination by implementation of DGT-SSETV-\u03bcCCP-OES as TRL4 on real samples;<\/li>\n<li>Demonstration of the utility and capability report for the new DGT-SSETV-\u03bcCCP-OES microanalytical methods for environment and food control quality;<\/li>\n<li>2 Internal Operating Procedures based on DGT-SSETV-\u03bcCCP-OES;<\/li>\n<li>National patent application;<\/li>\n<li>Dissemination of results through participation in scientific national and international events;<\/li>\n<li>Dissemination of results through papers in WoS indexed journals.<\/li>\n<\/ul>\n<p><strong>Project start<\/strong>: 27\/06\/2022<br \/>\n<strong>Project end<\/strong>: 26\/06\/2024<br \/>\n<strong>Project duration<\/strong>: 24 months<\/p>\n<h3>Partners:<\/h3>\n<ul>\n<li>P1 &#8211; BABES BOLYAI UNIVERSITY Cluj-Napoca<br \/>\nProject responsible: Prof. Dr. Tiberiu Fren\u021biu<\/li>\n<li>P2 \u2013 TECHNICAL UNIVERSITY OF CLUJ &#8211; NAPOCA<br \/>\nProject responsible: Prof. Dr. Dorin Petreu\u0219<\/li>\n<\/ul>\n<h3>Budget:<\/h3>\n<p><strong>Project budget<\/strong> 598.795,00 RON<br \/>\n<strong>Co-financing<\/strong>: 0,00 RON<\/p>\n<h3>Contact<\/h3>\n<p>Project coordinator<br \/>\nSenior Researcher I Dr. Marin Senila<br \/>\nStr. Donath nr. 67, Cluj-Napoca, Romania<br \/>\nE-mail: marin.senila@icia.ro; icia@icia.ro<br \/>\nTel\/Fax: +40 264 420590 \/ +40 264 667<\/p>\n<hr \/>\n<h3 style=\"font-weight: 400;\"><strong>Obtained results \u2013 Stage 1<\/strong><\/h3>\n<ol>\n<li>Testing and optimization of the working conditions for in-situ and ex-situ preconcentration of Hg, Pb, Cd, As, Sb, Se, Cu and Zn using the DGT devices<\/li>\n<li>Optimization report of the working conditions for DGT-SSETV-\u00b5CCP-OES equipment for Zn, Cd, Cu, Hg and Pb determination<\/li>\n<li>Development of specialized software to control the thermal program of the Rh filament (electrothermal evaporation of Zn, Cd, Cu, Hg and Pb)<\/li>\n<li>DGT-SSETV-\u03bcCCP-OES experimental model developed at TRL4<\/li>\n<li>Participatio at national scientific events<\/li>\n<\/ol>\n<p style=\"font-weight: 400;\"><u>Eniko Covaci<\/u>, Zsofia Sandor, Bogdan Simion Angyus, Marin Senila, Tiberiu Frentiu. Optical emission spectrometry by electrothermal vaporization in a capacitively coupled plasma microtorch as a specific detector in simultaneous multielemental passive sampling by diffusive\u00a0 gradients in thin films (DGT-SSETV-\u03bcCCP-OES): Preliminary studies on the optimization of working parameters. Conferin\u021ba Na\u021bional\u0103 de Chimie, edi\u021bia XXXVI, sec\u021biunea Chimie anorganic\u0103, chimie-fizic\u0103 \u0219i analitic\u0103, C\u0103lim\u0103ne\u0219ti-C\u0103ciulata, 04\u201307 octombrie 2022 &#8211; Oral communication<\/p>\n<p style=\"font-weight: 400;\">Zsofia Sandor, Eniko Covaci, Bogdan Simion Angyus, Marin Senila, <u>Tiberiu Frentiu<\/u>. Microanalytical method for monitoring of toxic elements in surface waters using passive sampling in diffusive gradients in thin films and detection by capacitively coupled plasma microtorch optical emission spectrometry with electrothermal vaporization\u00a0 (DGT-SSETV-\u03bcCCP-OES). Conferin\u021ba Na\u021bional\u0103 de Chimie, edi\u021bia XXXVI, sec\u021biunea Chimie anorganic\u0103, chimie-fizic\u0103 \u0219i analitic\u0103, C\u0103lim\u0103ne\u0219ti-C\u0103ciulata, 04\u201307 octombrie 2022 &#8211; Poster<\/p>\n<p><a href=\"https:\/\/icia.ro\/wp-content\/uploads\/2024\/06\/Stage1_EN.pdf\">Stage 1 report (PDF)<\/a><\/p>\n<hr \/>\n<h3>Obtained results \u2013 Stage 2<\/h3>\n<ul>\n<li>Optimization report of the working conditions for DGT-SSETV-\u00b5CCP-OES equipment for As, Sb and Se determination<\/li>\n<li>Experimental report on the improvement of analytical performance for DGT-SSETV-\u03bcCCP-OES methods with and without DGT sampling<\/li>\n<li>Comparative study of analytical performance of DGT-SSETV-\u03bcCCP-OES with traditional methods, GFAAS, TDAAS, ICP-OES and European Legislations<\/li>\n<li>Validation report of microanalytical methods based on DGT-SSETV-\u00b5CCP-OES for simultaneous multielemental determination in environmental samples<\/li>\n<li>Validation report of microanalytical methods based on DGT-SSETV-\u00b5CCP-OES for simultaneous multielemental determination in food samples<\/li>\n<li>specialized software to control the thermal program of the Rh filament (electrothermal evaporation of As, Sb and Se)<\/li>\n<li>Participation at scientific events &#8211; 8 participations at national si international condeference: 6 poster presentations and 2 oral presentation<\/li>\n<li>8. 3 papes published \/ submitted at WoS indexed journals<\/li>\n<\/ul>\n<h3>Participation at scientific events<\/h3>\n<p><strong>3 presentations at 49th International Conference of Slovak Society of Chemical Engineering (SSCHE), Tatranske Matliare, Slovacia, 15\u201318 May 2023<\/strong><\/p>\n<p>1. Eniko Covaci, Simion Bogdan Angyus, Marin Senila, Maria Frentiu, Tiberiu Frentiu. Elimination of spectral interference between Cd and As in their monitoring in water by using in-situ diffusive gradients in thin film passive sampling and detection by ex-situ microplasma optical emission spectrometry set-up equiped with a low-resolution microspectrometer. (Poster)<\/p>\n<p>2. Eniko Covaci, Simion Bogdan Angyus, Marin Senila, Maria Frentiu, Tiberiu Frentiu. Evaluation of green and white degree of a method based on in-situ diffusive gradients in thin film passive sampling coupled with ex-situ microplasma optical emission spectrometry set-up for determination of toxic elements in river water. (Poster)<\/p>\n<p>3. Simion Bogdan Angyus, Marin Senila, Eniko Covaci, Tiberiu Frentiu, Maria Frentiu. Monitoring of toxic trace metals in river water using in-situ diffusive gradients in thin film passive sampling and small-sized electrothermal vaporization capacitively coupled plasma microtorch optical emission spectrometry. (Poster)<\/p>\n<p><strong>2 presentations at 4th Young Researchers\u2019 International Conference on Chemistry and Chemical Engineering (YRICCCE IV), Debrecen, Ungaria, 1\u20133 June 2023<\/strong><\/p>\n<p>4. Simion Bogdan Angyus, Marin Senila, Eniko Covaci, Tiberiu Frentiu. Diffusive gradients in thin film and electrothermal vaporization capacitively coupled plasma optical emission spectroscopy method for the evaluation of bioavailable Cu, Zn, Cd and Pb fraction in agricultural soils (Oral presentation)<\/p>\n<p>5. Eniko Covaci, Simion Bogdan Angyus, Marin Senila, Maria Frentiu, Tiberiu Frentiu. Greenness and whiteness of small-sized electrothermal vaporization capacitively coupled plasma optical emission spectrometry with in-situ diffusive gradients in thin films passive sampling (DGT-SSETV-\u03bcCCP-OES) (Oral presentation)<\/p>\n<p><strong>One presentation at 14th International Conference Processes in Isotopes and Molecules, Cluj-Napoca, Romania, 19-22 September 2023<\/strong><\/p>\n<p>6. Sergiu Cadar, Dorin Petreus, Toma Patarau, Eniko Szilagyi, Bogdan Angyus, Frentiu Tiberiu, Optimization of the electrothermal evaporation process based on intelligent control of the power source. (Poster)<\/p>\n<p><strong>One presentation at IEEE 29th International Symposium for Design and Technology in Electronic Packaging (SIITME), Craiova, Romania. 17-21 October 2023<\/strong><\/p>\n<p>7. Sergiu Cadar, Dorin Petreus, Toma Patarau, Eniko Szilagyi. Comparative analysis of two types of filaments with COMSOL for electrothermal process. (Poster)<\/p>\n<p><strong>One presentation at the Conference Agriculture and Food &#8211; current and future challenges, AGRIFA, Cluj-Napoca, Romania. 20 October 2023<\/strong><\/p>\n<p>8. Marin Senila, Marius Roman, Bogdan Angyus. Mercury fractionation in soil using Diffusive Gradients in Thin-films coupled with thermal decomposition &#8211; atomic absorption spectrometry. (Poster)<\/p>\n<h4>Papers published \/ submitted for publication at WoS indexed journals<\/h4>\n<ol>\n<li>Simion Bogdan Angyus, Marin Senila, Tiberiu Frentiu, Michaela Ponta, Maria Frentiu, Eniko Covaci. In-situ Diffusive Gradients in thin-films passive sampling coupled with ex-situ small-sized electrothermal vaporization capacitively coupled plasma microtorch optical emission spectrometry as green and white method for the simultaneous determination of labile species of toxic elements in surface water. Talanta, 2023, 259, numar articol 124551, DOI: 10.1016\/j.talanta.2023.124551 (IF 6.1)<\/li>\n<li>Simion Bogdan Angyus, Marin Senila, Eniko Covaci, Michaela Ponta, Maria Frentiu, Tiberiu Frentiu. Simultaneous determination of Cd, Pb, Cu and Zn as total and labile fraction in soil using small-sized electrothermal vaporization capacitively coupled plasma microtorch optical emission spectrometry after diffusive gradients in thin-films passive accumulation. Journal of Analytical Atomic Spectrometry, accepted 2023, DOI: 10.1039\/D3JA00258F (IF 3.4)<\/li>\n<li>Marin Senila, Metals and metalloids monitoring in water by passive sampling: A review, Reviews in Analytical Chemistry, accepted 2023, DOI: 10.1515\/revac-2023-0065, (IF 4.3)<\/li>\n<\/ol>\n<p><a href=\"https:\/\/icia.ro\/wp-content\/uploads\/2024\/06\/Stage2_EN.pdf\">Stage 2 report (PDF)<\/a><\/p>\n<hr \/>\n<h3>Obtained results \u2013 Stage 3<\/h3>\n<ol>\n<li>Microanalytical methods developed for environmental samples (DGT-SSETV-\u03bcCCP-OES) TRL4<\/li>\n<li>Microanalytical methods developed for food samples (DGT-SSETV-\u03bcCCP-OES) TRL4<\/li>\n<li>Developed analytical methods based on DGT and classical methods for comparison with (DGT-SSETV-\u03bcCCP-OES)<\/li>\n<li>Report on the demonstration of the usefulness and functionality of the new microanalytical methods DGT-SSETV-\u03bcCCP-OES<\/li>\n<li>2 Standard operating procedures based on DGT-SSETV-\u03bcCCP-OES<\/li>\n<li>VP on intellectual property rights for industrial research<\/li>\n<li>National patent application<\/li>\n<li>3 Participation at scientific events &#8211; international conferences<\/li>\n<li>5 papers published at WoS indexed journals with IF&gt;3<\/li>\n<\/ol>\n<p><strong>Conference participations<\/strong><br \/>\n\u2022 <strong>2 Participations at the 50th International Conference of Slovak Society of Chemical Engineering (SSCHE), Tatranske Matliare, Slovakia, 20\u201324 May 2024<\/strong><br \/>\n1. S. Angyus, T. Frentiu, M. Frentiu, E. Covaci, M. Senila Evaluation of mercury concentration and mobility in soils around a former chlor-alkali plant using diffusive gradients in thin films (DGT) technique (Poster)<br \/>\n2. E. Covaci, S. Angyus, M. Senila, M. Frentiu, T. Frentiu Speciation of toxic metals in soil as total and labile fraction using diffusive gradients in thin films (DGT) passive sampling and determination by capacitively coupled plasma optical emission spectrometry (Poster)<br \/>\n\u2022 <strong>1 Participation at the International Spring Seminar on Electronics Technology, 15-19 May 2024, Prague, Czech Republic<\/strong><br \/>\n1. S. Cadar, D. Petreus, T. Patarau, E. Szilagyi Design of a flat coil electrothermal vaporization device for inductively coupled plasma optical emission spectrometry (Poster).<\/p>\n<p><strong>Published scientific articles<\/strong><br \/>\n1. M. Senila, M.A. Resz, L. Senila, I. Torok, Application of Diffusive Gradients in Thin-films (DGT) for assessing the heavy metals mobility in soil and prediction of their transfer to Russula virescens, Science of The Total Environment, 2024, 909, 168591 (FI = 9.8)<br \/>\n2. M. Senila, E. Kovacs, Use of diffusive gradients in thin-film technique to predict the mobility and transfer of nutrients and toxic elements from agricultural soil to crops\u2014an overview of recent studies, Environmental Science and Pollution Research, 2024 (FI = 5.8).<br \/>\n3. M. Senila, E.A. Levei, T. Frentiu, C. Mihali, S.B. Angyus, Assessment of mercury bioavailability in garden soils around a former nonferrous metal mining area using DGT, accumulation in vegetables, and implications for health risk. Environmental Monitoring and Assessment, 2023, 195, 1554 (FI = 3.0)<br \/>\n4. M. Senila, M.A. Resz, I. Torok, L. Senila, Nutritional composition and health risk of toxic metals of some edible wild mushrooms growing in a mining area of Apuseni Mountains, Western Carpathians, Journal of Food Composition and Analysis, 2024, 128, 106061 (FI = 4.3)<br \/>\n5. M. Senila, O. Cadar, T. Frentiu, L. Senila, S.B. Angyus, Diffusive Gradients in Thin-films as passive sampling tool for the measurement of labile species in fractionation analysis of metals (Fe, Mn, Cu, Zn and Pb) in beer, Microchemical Journal, 2024, 198, 2024, 110195 (IF = 4.8)<\/p>\n<p><a href=\"https:\/\/icia.ro\/wp-content\/uploads\/2024\/06\/Stage3_EN.pdf\">Stage 3 report (PDF)<\/a><\/p>\n<hr \/>\n<p><a href=\"https:\/\/icia.ro\/wp-content\/uploads\/2024\/06\/Final-report_EN.pdf\">Final report (PDF)<\/a><\/p>","protected":false},"excerpt":{"rendered":"<p>Project title: Simultaneous elemental microanalytical method for environment and food control using passive sampling coupled with miniaturized instrumentation based on plasma microtorch optical emission spectrometry Acronym: MULTIPASS Contract no: 733PED \/ 27.06.2022 Contracting Authority: Executive Agency for Higher Education, Research, Development and Innovation Funding (UEFISCDI), P2 &#8211; Increasing the competitiveness of the Romanian economy through [&hellip;]<\/p>\n","protected":false},"author":1,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":[],"acf":[],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v20.9 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>MULTIPASS - INCDO INOE 2000 ICIA<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/icia.ro\/multipass\/\" \/>\n<meta property=\"og:locale\" content=\"en_US\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"MULTIPASS - INCDO INOE 2000 ICIA\" \/>\n<meta property=\"og:description\" content=\"Project title: Simultaneous elemental microanalytical method for environment and food control using passive sampling coupled with miniaturized instrumentation based on plasma microtorch optical emission spectrometry Acronym: MULTIPASS Contract no: 733PED \/ 27.06.2022 Contracting Authority: Executive Agency for Higher Education, Research, Development and Innovation Funding (UEFISCDI), P2 &#8211; 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